Issue 5, 2005
From the journal:

New Journal of Chemistry

Synthesis of non-substituted phthalocyanines by standard and non-standard techniques. Influence of solvent nature in phthalocyanine preparation at low temperature by UV-treatment of the reaction system

B. I. Kharisov,*a   U. Ortiz Méndez,a   J. L. Almaraz Garzaa  and  J. R. Almaguer Rodrígueza  

* Corresponding authors

a Universidad Autónoma de Nuevo León, Monterrey, México
E-mail: bkhariss@ccr.dsi.uanl.mx

Abstract

Several synthetic techniques for metal-free phthalocyanines (Pc) and d- and f-metal phthalocyaninates (“PcM”) starting from different precursors (phthalonitrile, urea and phthalic anhydride, phthalimide, phthalic acid, etc.) are reviewed. Conventional methods are presented, as well as some less well-known techniques such as those using ultrasound, laser, microwaves, or nuclear transformation. Special attention is paid to phthalocyanine formation at relatively low temperatures (0–60 °C). Experimental results on Pc formation using UV-irradiation of the reaction system are presented.

Graphical abstract: Synthesis of non-substituted phthalocyanines by standard and non-standard techniques. Influence of solvent nature in phthalocyanine preparation at low temperature by UV-treatment of the reaction system

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Article information

DOI
https://doi.org/10.1039/B415712P
Article type
Paper
Submitted
11 Oct 2004
Accepted
24 Feb 2005
First published
16 Mar 2005

New J. Chem., 2005,29, 686-692

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Synthesis of non-substituted phthalocyanines by standard and non-standard techniques. Influence of solvent nature in phthalocyanine preparation at low temperature by UV-treatment of the reaction system

B. I. Kharisov, U. Ortiz Méndez, J. L. Almaraz Garza and J. R. Almaguer Rodríguez, New J. Chem., 2005, 29, 686 DOI: 10.1039/B415712P

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