Abstract
Nano-electromechanical systems implement the opto-mechanical interaction combining electromagnetic circuits and mechanical elements. We investigate an inductively coupled nano-electromechanical system, where a superconducting quantum interference device (SQUID) realizes the coupling. We show that the resonance frequency of the mechanically compliant string embedded into the SQUID loop can be controlled in two different ways: (1) the bias magnetic flux applied perpendicular to the SQUID loop, (2) the magnitude of the in-plane bias magnetic field contributing to the nano-electromechanical coupling. These findings are quantitatively explained by the inductive interaction contributing to the effective spring constant of the mechanical resonator. In addition, we observe a residual field dependent shift of the mechanical resonance frequency, which we attribute to the finite flux pinning of vortices trapped in the magnetic field biased nanostring.
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Introduction
The opto-mechanical interaction couples the displacement of a mechanical mode to the resonance frequency of an optical resonator. This setting is key for the realization of ultra-sensitive force detectors and the investigation of quantum mechanics in the literal sense1,2,3,4. One sub-field of common opto-mechanical systems is the field of circuit- or nano- electromechanical systems, where the role of the optical resonator, operating in the terahertz range, is taken over by a gigahertz microwave resonator. For the majority of devices, the opto-mechanical interaction is realized by capacitive coupling, where the displacement of the mechanical element is transduced into a variation of the microwave resonator capacitance, thereby shifting its resonance frequency5,6,7. Here, vacuum coupling rates have reached the widely reported limit of 300 Hz8,9,10,11 and effects such as ground state cooling12, strong coupling6,13, state transfer14, mechanical squeezing15, as well as electromechanically induced transparency effects7,16,17,18 have been reported. Only recently, the concept of inductive coupling, where the mechanical displacement is transduced into a change of the resonator inductance and hence resonance frequency, has been demonstrated19,20,21,22. This concept offers the potential to significantly increase the single-photon coupling rate \(g_0\) beyond the above-mentioned limit8,9,10,11,23. Devices realizing this concept are based on a direct-current superconducting quantum interference device (dc-SQUID), incorporated into a coplanar waveguide (CPW) microwave resonator. Here, the dc-SQUID can be viewed as a nonlinear, flux-controllable inductor. The integration of a mechanically compliant system into one arm of the dc-SQUID enables the opto-mechanical interaction. Notably, the mechanical element experiences a backaction fundamentally based on the Lorentz force19,23,24,25. This raises several interesting questions: (1) Is this effect present in circuit-integrated nano-electromechanical devices, (2) does it represent an efficient and fast way to tune the mechanical frequency, and (3) do the magnetic fields controlling the optomechanical interaction constant \(g_0\) affect the mechanical properties of the device. While the tuning of the mechanical frequency has been discussed for in-plane magnetic fields in Ref. 19 and has been linked exclusively to the Lorentz force, our measurements suggest a more complex behavior. In particular, we find evidence of a change of the string’s intrinsic mechanical properties when applying magnetic fields. With this motivation, we present experimental data of a nano-electromechanical system based on an inductive coupling scheme, where we explore the tuning of the mechanical resonance frequency as a function of multiple control parameters. In the experiment, we observe a flux-dependent shift of the mechanical resonance frequency, which we can quantitatively describe by theoretical predictions. Interestingly, we observe an additional, flux-independent shift of the mechanical frequency which we attribute to the influence of magnetic flux lines trapped in the superconducting nanostring.
Results and discussion
Device and concept
The device investigated in this letter is shown in Fig. 1a–c. A \(\lambda /4\) superconducting CPW resonator is short-circuited to ground via a dc-SQUID at one end (cf. Fig. 1b). The inductance of the SQUID is flux-dependent, allowing for the control of the resonance frequency via an out-of-plane oriented applied magnetic field \(B_\mathrm {OOP}\). To enable the electromechanical interaction, parts of the SQUID loop are suspended, forming two nanomechanical string oscillators (cf. Fig. 1c). The displacement of the strings modulates the effective area of the SQUID and therefore alters the magnetic flux threading the loop (cf. Fig. 1e). Since the inductance of the dc-SQUID depends on the applied flux, this in turn results in a modulation of the resonance frequency of the microwave resonator. An equivalent circuit representation of the device is presented in Fig. 1d), showing a LC-resonator with an additional variable inductance L(x), which is provided by the mechanically compliant SQUID and modulated by the time-varying displacement x(t) of the nanostring oscillators. We note that the nanostrings support both out-of-plane (OOP) and in-plane (IP) flexural modes. By applying a magnetic field parallel (perpendicular) to the chip plane, the circuit becomes sensitive to the OOP (IP) displacement of the nanostrings. In this experiment, we use a strong in-plane magnetic field \(B_\mathrm {IP}\) to realize an enhanced electromechanical interaction, since the in-plane field orientation supports a much higher critical magnetic field compared to the OOP direction26. Additionally, we employ a weak magnetic field \(B_\mathrm {OOP}\) to control the resonance frequency of the microwave resonator.
According to Ref. 23, the system can be described in terms of the mechanical displacement X and the center-of-mass coordinate \(\varphi _+ = (\phi _1+\phi _2)/2\) of the SQUID, where \(\phi _1\) and \(\phi _2\) are the phase differences across the Josephson junctions. The resulting Hamiltonian can be written as
here \(m_\mathrm {r}\) and \(\Omega _{\mathrm {m}}\) are the mass and the resonance frequency of the mechanical string, \(\Phi _0\) the flux quantum and \(E(\varphi _+,X)\) represents the potential energy of the dc-SQUID. As the resonance frequency of the microwave cavity, \(\omega _c\), is much larger than the mechanical resonance frequency (\(\omega _{\mathrm {c}}\gg \Omega _{\mathrm {m}}\)), the system operates in the dispersive limit and the mechanical displacement along with the corresponding flux change can be considered as static on the timescales relevant for the SQUID dynamics. In this limit, the SQUID can be approximated as a harmonic oscillator and an expansion of its potential energy in terms of the phase up to second order can be performed. The resulting phase-dependent terms describe the dynamic interaction of the electromechanical system, which eventually lead to a radiation pressure interaction term of the form \(H_\mathrm {int} = \hbar g_0 {\hat{a}}^\dagger {\hat{a}}({\hat{b}}^\dagger + {\hat{b}})\), where \({\hat{a}}\) and \({\hat{b}}\) denote the ladder operators of the microwave resonator and mechanical oscillator, respectively8,9,10,19,20. To investigate the mechanical resonance frequency, we instead focus on the phase-independent term in the expansion, which induces a static, but flux-dependent shift of the uncoupled mechanical resonance frequency \(\Omega _0\) towards an effective frequency \(\Omega _{\mathrm {m}}\). According to23, one obtains
here \(E_\mathrm {J} = \hbar (I_1+I_2)/4e\) is the SQUID average Josephson energy with \(I_{1,2}\) representing the critical currents of the individual Josephson junctions, l is the length of the string and \(\lambda\) its shape factor24. Furthermore, we have introduced \(S_0=\sqrt{\cos ^2(\phi _{\mathrm {b}})+\alpha ^2\sin ^2(\phi _{\mathrm {b}})}\) with the normalized bias flux \(\phi _\mathrm {b} = \pi \Phi _{\mathrm {b}}/\Phi _0\), which is generated by the control field \(B_\mathrm {OOP}\). The asymmetry parameter \(0< \alpha < 1\) accounts for non-identical Josephson junctions in the SQUID and is defined by \(I_1 = I_0(1-\alpha )\) and \(I_2 = I_0(1+\alpha )\) with the average critical current \(I_0 = (I_1 + I_2)/2\).
The modification of the mechanical resonance frequency reflected in Eq. (2) can be understood as a consequence of a total Lorentz force \(F_\mathrm {L} = B_\mathrm {IP}lI(\Phi )\) originating from the flux-dependent circulating current \(I(\Phi )\) of the dc-SQUID. However, as the area of the SQUID perpendicular to \(B_\mathrm {IP}\) and therefore the total flux \(\Phi\) is modulated by the mechanical motion of the nanostring (cf. Fig 1e), a displacement-dependent restoring force is obtained. This corresponds to an effective change in the strings stiffness and hence a modification of the mechanical resonance frequency. Note that this type of backaction is different from the shift in \(\Omega _{\mathrm {m}}\) caused by the opto-mechanical interaction2,27.
The device depicted in Fig. 1a–c is fabricated using standard nanofabrication techniques, double-layer shadow evaporation of aluminium and reactive ion etching on high resistivity silicon (see Ref. 20 for the fabrication details of this particular device). The suspended nanostrings have dimensions of \((l,w,t) = (20,0.2,0.11)\,{\upmu \mathrm{m}}\), resulting in an effective mass of \(m_\mathrm {r} ={0.6}\,\mathrm{{pg}}\) and mechanical out-of-plane frequencies of \(\Omega _{\mathrm {m}}/2\pi \approx {5.8}\,\mathrm{{MHz}}\) at millikelvin temperatures.
Device characterization
We start with the characterization of the flux-tunable CPW resonator using microwave transmission measurements. We record the frequency dependent complex transmission using a vector network analyzer for various OOP flux bias values \(\Phi _{\mathrm {b}}\). The results are shown in Fig. 2a for \(B_\mathrm {IP} = 0\). The resonance frequency of the microwave resonator, \(\omega _{\mathrm {c}}\), is visible as a dark blue feature in the color-coded scattering parameter \(|S_{21}|^2\). We observe a maximum frequency of \(\omega _{\mathrm {c}}/2\pi \approx {7.45}\,\mathrm{{GHz}}\), which decreases as \(\Phi _{\mathrm {b}}\) is increased due to the increasing Josephson inductance of the SQUID. This effect is periodic in \(\Phi _{\mathrm {b}}\) as expected for such resonators19,20,28,29 and allows for the experimental control of the resonance frequency over a range of roughly \({750}\,\mathrm{{MHz}}\). In zero-(OOP)-field we find a total linewidth of \(\kappa /2\pi \approx {2.5}\,\mathrm{{MHz}}\) and a minimum Josephson inductance of the SQUID \(L_\mathrm {J} = {0.36}\,\mathrm{{nH}}\). A more detailed analysis of this device is presented in Ref. 20.
In order to investigate the impact of the electromechanical system on the mechanical subsystem’s frequency, we analyze the properties of the mechanical resonator as function of \(\Phi _{\mathrm {b}}\) and the in-plane bias field \(B_\mathrm {IP}\). To this end, we record a thermal displacement spectrum of the anti-Stokes field as illustrated in Fig. 2b. In detail, we inject a weak probe tone, which is resonant with the microwave resonator [\(\omega _\mathrm {p} = \omega _{\mathrm {c}}(\Phi _{\mathrm {b}})\)]. In addition, a second, weaker stabilizer tone is applied at \(\omega _\mathrm {stab} = \omega _{\mathrm {c}}(\Phi _{\mathrm {b}})+{500}\,\mathrm{{kHz}}\) (not shown). The transmission of the stabilizer tone constitutes the error signal input used for the active feedback provided via \(B_\mathrm {OOP}\) to counteract any magnetic field fluctuations. We use tones with small detuning and ultra-low powers (\(P_\mathrm {stab}< P_\mathrm {probe} < {2}{fW}\)) to avoid opto-mechanical heating and cooling effects as well as the resulting frequency shift (opto-mechanical spring effect)2,20,27.
The thermal displacement noise of the nanostring modulates the inductance of the SQUID and thus \(\omega _{\mathrm {c}}\). The resulting sidebands, which correspond to the Stokes and anti-Stokes field, appear at \(\omega _\mathrm {p} \pm \Omega _{\mathrm {m}}(\Phi _\mathrm {b})\). We downconvert the signal at \(\omega _c(\Phi _\mathrm {b}) + {3.5}\,\mathrm{{MHz}}\) and selectively record the spectral density of the anti-Stokes field. The data can then be fitted with a Lorentzian lineshape to characterize the mechanical oscillator. We extract the mechanical resonance frequency \(\Omega _{\mathrm {m}}/2\pi \approx {5.8}\,\mathrm{{MHz}}\) and the linewidth \(\Gamma _\mathrm {m}/2\pi \approx {20}\,\mathrm{{Hz}}\), corresponding to \(Q \approx {290000}\). Based on Eq. (2) we expect an evolution of \(\Omega _{\mathrm {m}}\) with \(B_\mathrm {OOP}\) or flux bias \(\Phi _{\mathrm {b}}\). Fig. 2c shows the recorded voltage power spectral density for various flux bias points and a fixed \(B_\mathrm {IP}\) of \({35}\,\mathrm{{mT}}\). Similar to the behavior of the microwave resonator, the mechanical frequency appears to decrease with an increasing flux bias applied to the SQUID.
Mechanical frequency control
To gain a deeper understanding of the effects at play, we perform the previously described experiment at various flux bias points \(\Phi _{\mathrm {b}}\) covering the full periodicity of the microwave resonator frequency. In addition, we repeat these flux sweeps for various in-plane magnetic fields ranging from 6.2 to 35 mT. The extracted mechanical resonance frequencies are plotted in Fig. 3. We note that the electromechanical coupling is strongly suppressed at small flux bias (\(|\Phi _\mathrm {b}/\Phi _0| < 0.1\)). Therefore, to verify the data in this regime, a piezoelectric actuator attached to the sample was used to resonantly drive the mechanical motion and increase the signal strength.
As shown in Fig. 3, the mechanical resonance frequency \(\Omega _{\mathrm {m}}\) approximately shows a parabolic tuning behavior with respect to the applied flux bias. We observe a maximum tuning of roughly 1 kHz at the maximum applied in-plane field, \(B_\mathrm {IP} = {35}\,\mathrm{{mT}}\). We compare these results with the theoretical prediction by fitting the data to Eq. (2), choosing \(E_\mathrm {J}\) and \(\Omega _0\) as the only free fit parameters. The SQUID asymmetry is fixed to a small value of \(\alpha = 1\%\) to account for minor fabrication deviations of the Josephson junctions, while the remainder of the device parameters has been determined in previous experiments20 and are summarized in Supplementary Table 1. The resulting model precisely describes our experimental findings, confirming the hypothesis that the shift of the mechanical resonance frequency is indeed caused by the Lorentz force acting on the nanostring within the SQUID. The good reproduction of the data by the model also suggests that the mechanical resonance frequency can be tuned quasi-continuously to any point described by Eq. (2). However, an analysis of the determined fit parameters (see inset) reveals that the uncoupled resonance frequency \(\Omega _\mathrm {0}\) increases by several hundred Hz as \(B_\mathrm {IP}\) is increased, an effect that is not accounted for by the theoretical description of the electromechanical system [cf. Eq. (2)]. We want to emphasize the distinction between this unpredicted shift in \(\Omega _0\) and the frequency tuning behaviour attributed to the Lorentz force: The change in mechanical frequency depending on the bias flux \(\Phi _{\mathrm {b}}\) penetrating the SQUID loop, as measured and modelled in Fig. 3, is well understood as a consequence of the Lorentz force acting on the oscillating nanostring. It can be described either by Eq. (2) or using a slightly different derivation as found in Ref. 19. Both descriptions share the same physical origin, i.e. a change in the SQUIDs circulating current due to the displacement of a mechanical element, which in turn experiences an effective spring stiffening. Our study of the mechanical resonance frequency as function of the in-plane bias field and the bias flux controlling the inductance of the SQUID allows us to quantitatively account for this Lorentz force based mechanism. Comparing this quantitative model with our experimental data, we can distinguish and extract the additional, field-dependent frequency shift \(\Delta \Omega _0\) (Fig. 3 inset), which is not accounted for by either of the above mentioned theoretical models.
Discussion of the additional frequency shift
Confronted with the unknown physical origin of this additional effect, we discuss various scenarios which could explain the \(B_\mathrm {IP}\)-dependence of \(\Omega _0\). One possible mechanism could be the volume change of the superconducting aluminium as the in-plane field approaches its critical field30. However, the commonly reported length changes on the order of \(\Delta V/V \approx 10^{-8}\) are too small to explain the observed frequency shifts \(\Delta \Omega _{\mathrm {m}}/\Omega _{\mathrm {m}}\approx 10^{-4}\). Higher order contributions to the opto-mechanical interaction, specifically the quadratic opto-mechanical coupling, would result in a \(B_\mathrm {IP}^2\)-dependence of \(\Omega _{\mathrm {m}}\)31. However, for our device parameters, we expect a frequency shift on the order of a few Hz and hence refrain from this conjecture. We also consider that the flux captured by the SQUID loop and the corresponding magnetic moment could give rise to a modification of the mechanical frequency if the device acts as a torque magnetometer32,33,34,35. However, controlling the number of flux quanta in the SQUID loop via \(B_\mathrm {OOP}\) allows us to rule out this conjecture (for details see Supplementary Note 2).
Finally, we draw parallels to vibrating reed experiments, which were able to measure the stiffness of the flux line lattice (FLL) in type-II superconductors and its influence on mechanical properties36,37. In particular, the FLL can exhibit quasi-elastic properties, couple to the motion of the atomic lattice and hence influence the mechanical resonance frequency. The strength of this coupling is quantified by the Labusch parameter \(\alpha _\mathrm {L}(B,T)\). Notably, in the case of very thin superconductors, as used for our experiment, the expected frequency change is \(\Omega ^2 = \Omega _0^2 + \alpha _L(B)/\rho\)37. The field-dependence of \(\alpha _\mathrm {L}(B)\) exhibits a power-law behavior \(\alpha _\mathrm {L}(B) \propto B^k\) where k can vary significantly across materials. While we are not aware that this effect has been reported for aluminium, sufficiently thin aluminium films can behave in ways characteristic of type-II superconductors38,39. Studies of other type-II superconductors find a range of \(k \approx 2 \pm 0.5\) and \(\alpha _\mathrm {L} \approx {10^{12}}\) to \(10^{15}\;{\text{N}}/{\text{m}}^{4}\)37,40,41. Fitting our experimental data with a power-law (Fig. 3 inset) we find \(\alpha _\mathrm {L} \propto B_\mathrm {IP}^{1.81}\) and \(\alpha _{{\text{L}}} (35\;{\text{mT}}) = 7.88\times 10^{14}\;{\text{N}}/{\text{m}}^{4}\), showing agreement with the reported values. While this suggests that flux line pinning is at the origin of the mechanical frequency shift, further investigations are warranted to fully confirm this hypothesis.
Conclusion
In summary, we present a detailed study of frequency tuning effects on a nanostring in an electromechanical system. We find a pronounced shift (\(> 50\, \Gamma _\mathrm {m}\)) in the mechanical resonance frequency as function of the flux bias condition of the SQUID. This \(\Phi _{\mathrm {b}}\)-dependent frequency shift is distinct from frequency shifts based on the opto-mechanical interaction and is quantitatively explained by an interaction induced by the SQUID via the Lorentz force. The ability to shift the mechanical resonance frequency using the flux bias of the SQUID allows for fast in-situ frequency modulation, which could be employed e.g. for parametric driving of the mechanical element. Furthermore, our detailed modelling reveals a previously unobserved field-dependent frequency shift that we attribute to the additional mechanical stiffness induced by the flux line lattice in the aluminium nanostring. This underlines the mechanical sensing capabilities of nanostrings and their potential applications in material science. The reduced size of this particular system promises a path to the investigation of the mechanical properties of few or individual flux lines. The detailed understanding of the frequency shifts, as it is presented in this work, is of utmost importance for applications relying on the precise in-situ control of the mechanical resonator frequency.
Methods
Microwave setup
All experiments are performed in a dilution refrigerator at a temperature of approximately \({85}\,\mathrm{{mK}}\) using spectroscopy schemes such as microwave transmission experiments and thermal sideband noise spectroscopy. A detailed description of the microwave detection setup can be found in Ref. 20.
Packaging and magnetic field control
To apply the strong in-plane and the weak out-of-plane magnetic field to the nano-electromechanical circuit, we position the chip in a superconducting solenoid magnet and mount a small superconducting coil on the sample enclosure. While the IP superconducting solenoid is used to apply fields of up to 35mT, the field provided by the OOP coil is limited to 1 mT. In order to achieve undisturbed exposure of the device to \(B_\mathrm {IP}\), we operate without magnetic shielding. As a consequence, the device is subject to fluctuations in the static magnetic field which are actively compensated by a feedback loop using the OOP coil as control entity.
Data availibility
Experimental data are available upon reasonable request at the corresponding author.
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Acknowledgements
This project has received funding from the European Union’s Horizon 2020 research and innovation program under Grant agreement No 736943 and from the Deutsche Forschungsgemeinschaft (DFG, German Research Foundation) under Germany’s Excellence Strategy-EXC-2111-390814868. A.S. acknowledges funding from ICREA Academia, Generalitat de Catalunya. We gratefully acknowledge valuable scientific discussions with D. Koelle.
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P.S. designed and fabricated the sample. T.L. performed the experiments. H.H., T.L. and P.S. built the measurement setup. T.L. performed theoretical modeling and analysis of the data. A.S. provided theoretical support to the interpretation of the data. T.L and H.H wrote the paper. H.H. and R.G. conceived the experiment. F.D. and A.M. supported the SQUID fabrication. H.H., R.G., F.D. and A.M. supervised the project. All authors discussed the results and contributed to the manuscript.
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Luschmann, T., Schmidt, P., Deppe, F. et al. Mechanical frequency control in inductively coupled electromechanical systems. Sci Rep 12, 1608 (2022). https://doi.org/10.1038/s41598-022-05438-x
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DOI: https://doi.org/10.1038/s41598-022-05438-x
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